Synthesis of poly(urethane-urea) varnish bearing azobenzene chromophoric pendants
Identifieur interne : 000568 ( Main/Exploration ); précédent : 000567; suivant : 000569Synthesis of poly(urethane-urea) varnish bearing azobenzene chromophoric pendants
Auteurs : Constantin Gaina [Roumanie] ; Viorica Gaina [Roumanie] ; Mariana Cristea [Roumanie]Source :
- Polymer Bulletin [ 0170-0839 ] ; 2012.
English descriptors
- Teeft :
- Aromatic proton, Azobenzene, Azobenzene chromophore, Azobenzene side group, Azobenzene unit, Chain extender, Chem, Chromophore, Contact angle, Contact angle measurement, Diethylene glycol, Dynamic contact angle, External structure, Gaina, Glass plate, Glass storage modulus, Glass transition, Glass transition temperature, Heating rate, Height image, Imidic monomer, Literature procedure, Maleimide, Maleimide chromophore, Modulus, Monomer, Nonlinear optical property, Onset temperature, Polym, Polym mater, Polymer, Polymer film, Polymeric material, Polyurethane, Polyurethane film, Pure appl chem, Room temperature, Soft segment, Storage modulus, Substitution reaction, Surface roughness, Vacuum oven, Varnish, Weight ratio.
Abstract
Abstract: A new diol with azoaromatic pendant was prepared by N-phenyl-4-amido-3,4-dichloromaleimide with 2-mercaptoethanol in the presence of NaOH, and used to obtain photosensible poly(urethane-urea) varnish. A poly(urethane-urea) varnish bearing azobenzene chromophores, based on a poly(ethylene adipate)diol (average molecular weight—2000), 4,4′-dibenzyldiisocyanate, diethylene glycol, trimethylolpropane, and afore-mentioned diol, were prepared and characterized. The polymers were characterized by FTIR spectroscopy, thermal analysis (DMA, DSC, and TGA), and the photochromic behavior by UV irradiation of thin films was discussed.
Url:
DOI: 10.1007/s00289-011-0543-7
Affiliations:
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Le document en format XML
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<term>Azobenzene unit</term>
<term>Chain extender</term>
<term>Chem</term>
<term>Chromophore</term>
<term>Contact angle</term>
<term>Contact angle measurement</term>
<term>Diethylene glycol</term>
<term>Dynamic contact angle</term>
<term>External structure</term>
<term>Gaina</term>
<term>Glass plate</term>
<term>Glass storage modulus</term>
<term>Glass transition</term>
<term>Glass transition temperature</term>
<term>Heating rate</term>
<term>Height image</term>
<term>Imidic monomer</term>
<term>Literature procedure</term>
<term>Maleimide</term>
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<term>Monomer</term>
<term>Nonlinear optical property</term>
<term>Onset temperature</term>
<term>Polym</term>
<term>Polym mater</term>
<term>Polymer</term>
<term>Polymer film</term>
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<term>Polyurethane</term>
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<term>Room temperature</term>
<term>Soft segment</term>
<term>Storage modulus</term>
<term>Substitution reaction</term>
<term>Surface roughness</term>
<term>Vacuum oven</term>
<term>Varnish</term>
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<front><div type="abstract" xml:lang="en">Abstract: A new diol with azoaromatic pendant was prepared by N-phenyl-4-amido-3,4-dichloromaleimide with 2-mercaptoethanol in the presence of NaOH, and used to obtain photosensible poly(urethane-urea) varnish. A poly(urethane-urea) varnish bearing azobenzene chromophores, based on a poly(ethylene adipate)diol (average molecular weight—2000), 4,4′-dibenzyldiisocyanate, diethylene glycol, trimethylolpropane, and afore-mentioned diol, were prepared and characterized. The polymers were characterized by FTIR spectroscopy, thermal analysis (DMA, DSC, and TGA), and the photochromic behavior by UV irradiation of thin films was discussed.</div>
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